Contents - Materials Manual M 46-01

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ContentsAggregateProcedureNumberOwnerFieldInUse ManualTest MethodT 11AASHTOT 19AASHTOT 21AASHTOOrganic Impurities in Fine Aggregates for ConcreteT 27AASHTOSieve Analysis of Fine and Coarse AggregatesT 27 T 11 WAQTCMaterials Finer Than 0.075 mm (No. 200) Sieve in MineralAggregates by WashingüüüüBulk Density (“Unit Weight”) and Voids in Aggregate (Rodding ProcedureOnly) (Checklist Only)FOP for AASHTO T 27 T 11, Sieve Analysis of Fine and CoarseAggregatesT 37AASHTOSieve Analysis of Mineral Filler for Hot Mix Asphalt (HMA)R 76AASHTOReducing Samples of Aggregate to Testing SizeR 76WAQTCT 84AASHTOSpecific Gravity and Absorption of Fine AggregatesT 85AASHTOSpecific Gravity and Absorption of Coarse AggregateT 85WAQTCR 90AASHTOR 90WAQTCT 96AASHTOT 112AASHTOT 113WSDOTT 123WSDOTT 125WSDOTT 126WSDOTSOP 128WSDOTT 176AASHT0T 176WAQTCT 255AASHTOT 255WAQTCT 288AASHTOT 289AASHTODetermining pH of Soil for Use in Corrosion TestingT 304AASHTOUncompacted Void Content of Fine AggregateT 304WAQTCT 335AASHTOWSDOT Materials ManualMay 2021üüüüFOP for AASHTO R 76, Reducing Samples of Aggregate to Testing SizeFOP for AASHTO T 85, Specific Gravity and Absorption of CoarseAggregateSampling Aggregate ProductsüüFOP for AASHTO R 90, Sampling Aggregate ProductsResistance to Degradation of Small-Size Coarse Aggregate by Abrasionand Impact in the Los Angeles MachineüüüüüüüClay Lumps and Friable Particles in AggregateüSampling for Aggregate Source ApprovalMethod of Test for Determination of Degradation ValueMethod of Test for Bark MulchDetermination of Fiber Length Percentages in Wood Strand MulchDetermination of Fiber Length Percentages in Hydraulically-AppliedErosion Control ProductsPlastic Fines in Graded Aggregates and Soils by Use of theSand Equivalent TestüüFOP for AASHTO T 176, Plastic Fines in Graded Aggregates and Soils bythe Use of the Sand Equivalent TestTotal Evaporable Moisture Content of Aggregate by DryingüüüFOP for AASHTO T 255, Total Evaporable Moisture Content of Aggregateby DryingüDetermining Minimum Laboratory Soil Resistivity (Checklist Only)üFOP for AASHTO T 304, Uncompacted Void Content of Fine AggregateDetermining the Percentage of Fracture in Coarse AggregateM 46-01.39Page 1 of 22

ContentsAggregateProcedureNumberOwnerT 335WAQTCT 417WSDOTT 716WSDOTFieldInUse ManualüüTest MethodüFOP for AASHTO T 335, Determining the Percentage of Fracture inCoarse AggregateüMethod of Test for Determining Minimum Resistivity and pH of Soiland WaterüMethod of Random Sampling for Locations of Testing and Sampling SitesBituminous CementProcedureNumberOwnerFieldInUse ManualTest MethodR 28AASHTOStandard Practice for Accelerated Aging of Asphalt Binder Using aPressurized Aging VesselR 29AASHTOStandard Practice for Grading or Verifying the Performance Grade (PG) ofan Asphalt BinderT 44AASHTOSolubility of Bituminous MaterialsT 48AASHTOFlash and Fire Points by Cleveland Open CupT 49AASHTOPenetration of Bituminous MaterialsT 50AASHTOFloat Test for Bituminous MaterialsT 51AASHTODuctility of Asphalt MaterialsT 53AASHTOSoftening Point of Bitumen (Ring-and-Ball Apparatus)T 59AASHTOEmulsified AsphaltsR 66AASHTOSampling Asphalt MaterialsR 66WAQTCE 70ASTMpH of Aqueous Solutions With the Glass ElectrodeT 72AASHTOSaybolt ViscosityT 228AASHTOSpecific Gravity of Semi-Solid Asphalt MaterialsT 240AASHTOEffect of Heat and Air on a Moving Film of Asphalt Binder(Rolling Thin-Film Oven Test)T 301AASHTOElastic Recovery Test of Asphalt Materials by Means of a DuctilometerT 313AASHTODetermining the Flexural Creep Stiffness of Asphalt Binder Using theBending Beam Rheometer (BBR)T 315AASHTODetermining the Rheological Properties of Asphalt Binder Usinga Dynamic Shear Rheometer (DSR)T 316AASHTOViscosity Determination of Asphalt Binder Using Rotational ViscometerSOP 318WSDOTT 350AASHTOT 426WSDOTD 3111ASTMPage 2 of 22üüüFOP for AASHTO R 66, Sampling Asphalt MaterialsStandard Operating Procedure for Melting of Flexible BituminousPavement Marker Adhesive for EvaluationMultiple Stress Creep Recovery (MSCR) Test of Asphalt Binder Using aDynamic Shear Reheometer (DSR)üPull-Off Test for Hot Melt Traffic Button AdhesiveFlexibility Determination of Hot-Melt Adhesives by Mandrel BendTest MethodWSDOT Materials Manual M 46-01.39May 2021

ContentsAsphalt MixtureProcedureNumberOwnerFieldInUse ManualTest MethodR 30AASHTOStandard Practice for Mixture Conditioning of Hot Mix Asphalt (HMA)T 30AASHTOMechanical Analysis of Extracted AggregateT 30WAQTCTM 14WAQTCT 37AASHTOSieve Analysis of Mineral Filler of Hot Mix Asphalt (HMA)R 47AASHTOReducing Samples of Asphalt Mixtures to Testing SizeR 47WAQTCR 79AASHTOR 79WAQTCR 96AASHTOInstallation, Operation, and Maintenance of Ignition FurnacesR 97AASHTOSampling Asphalt MixturesR 97WAQTCT 166AASHTOT 166WAQTCT 209AASHTOT 209WAQTCT 269AASHTOPercent Air Void in Compacted Dense and Open Asphalt MixturesT 308AASHTODetermining the Asphalt Binder Content of Asphalt Mixtures by the IgnitionMethodT 308WAQTCT 312AASHTOT 312WSDOTT 324AASHTOT 329AASHTOT 329WAQTCT 331AASHTOT 331WAQTCT 355AASHTOT 355WAQTCüüFOP for AASHTO T 355, In-Place Density of Asphalt Mixtures byNuclear MethodsT 716WSDOTüüMethod of Random Sampling for Locations of Testing and Sampling SitesWSDOT Materials ManualMay 2021üüüüüFOP for AASHTO T 30, Mechanical Analysis of Extracted AggregateLaboratory Prepared Asphalt Mixture SpecimensFOP for AASHTO R 47, Reducing Samples of Asphalt Mixtures toTesting SizeVacuum Drying Compacted Asphalt SpecimensüüüüFOP for AASHTO R 79, Vacuum Drying Compacted Asphalt SpecimensFOP for AASHTO R 97, Sampling of Asphalt MixturesBulk Specific Gravity (Gmb) of Compacted Asphalt Mixtures UsingSaturated Surface-Dry SpecimensüüFOP for AASHTO T 166, Bulk Specific Gravity (Gmb) of Compacted AsphaltMixtures Using Saturated Surface-Dry SpecimensTheoretical Maximum Specific Gravity (Gmm) and Density ofAsphalt MixturesüüüüFOP for AASHTO T 209, Theoretical Maximum Specific Gravity (Gmm) andDensity of Asphalt MixturesFOP for AASHTO T 308, Determining the Asphalt Binder Content ofAsphalt Mixtures by the Ignition MethodPreparing and Determining the Density of Asphalt Mixture Specimens byMeans of the Superpave Gyratory CompactorüüFOP for AASHTO T 312, Preparing and Determining the Density of AsphaltMixture Specimens by Means of the Superpave Gyratory CompactorüHamburg Wheel-Track Testing of Compacted Asphalt MixturesMoisture Content of Asphalt Mixtures by Oven MethodüüFOP for AASHTO T 329, Moisture Content of Asphalt Mixtures byOven MethodBulk Specific Gravity (Gmb) and Density of Compacted Asphalt MixturesUsing Automatic Vacuum Sealing MethodüüFOP for AASHTO T 331, Bulk Specific Gravity (Gmb) and Density ofCompacted Asphalt Mixtures Using Automatic Vacuum Sealing MethodIn-Place Density of Asphalt Mixtures by Nuclear MethodsM 46-01.39Page 3 of 22

ContentsAsphalt MixtureProcedureNumberOwnerT 720WSDOTSOP 729WSDOTSOP 730FieldInUse ManualTest MethodüMethod of Test for Thickness Measurement of Hot Mix Asphalt(HMA) CoresüüStandard Operating Procedure for Determination of the Moving Average ofTheoretical Maximum Density (TMD) for HMAWSDOTüüStandard Operating Procedure for Correlation of Nuclear Gauge DensitiesWith Hot Mix Asphalt (HMA) CoresSOP 731WSDOTüüStandard Operating Procedure for Determining Volumetric Properties ofHot Mix AsphaltSOP 732WSDOTüüStandard Operating Procedure for Volumetric Design for Hot-Mix Asphalt(HMA)SOP 733WSDOTüüStandard Operating Procedure for Determination of PavementDensity Differentials Using the Nuclear Density GaugeSOP 734WSDOTüüStandard Operating Procedure for Sampling Hot Mix AsphaltAfter Compaction (Obtaining Cores)SOP 735WSDOTüStandard Operating Procedure for Longitudinal Joint DensitySOP 736WSDOTSOP 737WSDOTD 6931ASTMüüüüPage 4 of 22In-Place Density of Bituminous Mixes Using CoresProcedure for the Forensic Testing of HMA Field CoresIndirect Tensile (IDT) Strength of Asphalt MixturesWSDOT Materials Manual M 46-01.39May 2021

ContentsCementProcedureNumberOwnerFieldInUse ManualTest MethodT 105AASHTOChemical Analysis of Hydraulic CementT 106AASHTOCompressive Strength of Hydraulic Cement Mortars (Using 50-mm or 2-in.Cube Specimens)T 106WSDOTT 107AASHTOAutoclave Expansion of Hydraulic CementT 129AASHTOAmount of Water Required for Normal Consistency of HydraulicCement PasteT 131AASHTOTime of Setting of Hydraulic Cement by Vicat NeedleT 133AASHTODensity of Hydraulic CementT 137AASHTOAir Content of Hydraulic Cement MortarT 153AASHTOFineness of Hydraulic Cement by Air Permeability ApparatusT 162AASHTOMechanical Mixing of Hydraulic Cement Pastes and Mortars ofPlastic ConsistencyT 260AASHTOSampling and Testing for Chloride Ion in Concrete and ConcreteRaw MaterialsT 303AASHTOAccelerated Detection of Potentially Deleterious Expansion of Mortar BarsDue to Alkali-Silica ReactionT 313WSDOTT 314WSDOTT 413WSDOTT 813WSDOTT 814WSDOTC 939WSDOTWSDOT Materials ManualMay 2021üüüüFOP for AASHTO for Compressive Strength of Hydraulic Cement Mortars(Using 2-in. or (50-mm) Cube Specimens)üüüMethod of Test for Cement-Latex CompatibilityüField Method of Fabrication of 2 in (50 mm) Cube Specimensfor Compressive Strength Testing of Grouts and MortarsüMethod of Test for Water Retention Efficiency of Liquid MembraneForming Compounds and Impermeable Sheet Materials forCuring ConcreteüFOP for ASTM for Flow of Grout for Preplaced-Aggregate Concrete (FlowCone Method)M 46-01.39Method of Test for Photovolt ReflectanceMethod of Test for Evaluating Waterproofing Effectiveness of Membraneand Membrane-Pavement SystemsPage 5 of 22

ContentsChemicalProcedureNumberOwnerFieldInUse ManualTest MethodLRFDCONSAASHTOSection 18, Bearing DevicesM 111AASHTOZinc (Hot-Dip Galvanized) Coatings on Iron and Steel ProductsM 251AASHTOPlain and Laminated Elastomeric Bridge BearingsT 65AASHTOMass (Weight) of Coating on Iron and Steel Articles With Zinc or Zinc-AlloyCoatingsT 105/C114AASHTOChemical Analysis of Hydraulic CementT 260AASHTOSampling and Testing for Chloride Ion in Concrete and Concrete RawMaterialsT 267AASHTODetermination of Organic Content in Soils by Loss on IgnitionC 109ASTMCompressive Strength of Hydraulic Cement Mortars (Using 2-in. or[50 mm] Cube Specimens)C 311ASTMSampling and Testing Fly Ash or Natural Pozzolans for Use in PortlandCement ConcreteC 579ASTMCompressive Strength of Chemical-Resistant Mortars, Grouts, MonolithicSurfacings, and Polymer ConcretesC 881ASTMStandard Specification for Epoxy-Resin-Base Bonding Systemsfor ConcreteC 882ASTMD 638ASTMTensile Properties of PlasticsD 695ASTMCompressive Properties of Rigid PlasticsD 792ASTMDensity and Specific Gravity (Relative Density) of Plastics byDisplacementD 1751ASTMPreformed Expansion Joint Filler for Concrete Paving and StructuralConstruction (Nonextruding and Resilient Bituminous Types)D 2240ASTMRubber Property-Durometer HardnessD 2628/M 220ASTMD 5167ASTMMelting of Hot-Applied Joint and Crack Sealant and Filler for EvaluationD 5329ASTMSealants and Fillers, Hot-Applied, for Joints and Cracks in AsphaltPavements and Portland Cement Concrete PavementsD 6690ASTMJoint and Crack Sealants, Hot Applied, for Concrete and AsphaltPavementsD 7091ASTMPage 6 of 22üüüüBond Strength of Epoxy-Resin Systems Used With Concrete By SlantShearPreformed Polychloroprene Elastomeric Joint Seals for ConcretePavementsNondestructive Measurement of Dry Film Thickness of NonmagneticCoatings Applied to Ferrous Metals and Nonmagnetic, NonconductiveCoatings Applied to Non-Ferrous MetalsWSDOT Materials Manual M 46-01.39May 2021

ContentsConcreteProcedureNumberOwnerFieldInUse ManualTest MethodTM 2WAQTCT 22AASHTOT 22WSDOTT 23AASHTOT 23WAQTCT 24AASHTOObtaining and Testing Drilled Cores and Sawed Beams of ConcreteR 39AASHTOStandard Practice for Making and Curing Concrete Test Specimens in theLaboratoryT 106AASHTOCompressive Strength of Hydraulic Cement Mortars (Using 50-mm or 2-in.Cube Specimens)T 106WSDOTT 119AASHTOT 119WAQTCT 121AASHTOT 121WAQTCC 140ASTMSampling and Testing Concrete Masonry Units and Related UnitsT 141AASHTOSampling Freshly Mixed ConcreteT 152AASHTOAir Content of Freshly Mixed Concrete by the Pressure MethodT 152WAQTCT 196AASHTOT 197AASHTOTime of Setting of Concrete Mixtures by Penetration ResistanceT 198AASHTOSplitting Tensile Strength of Cylindrical Concrete SpecimensT 231AASHTOCapping Cylindrical Concrete SpecimensT 231WSDOTT 260AASHTOSampling and Testing for Chloride Ion in Concrete and ConcreteRaw MaterialsT 277AASHTOElectrical Indication of Concrete’s Ability to Resist Chloride Ion PenetrationT 309AASHTOTemperature of Freshly Mixed Portland Cement ConcreteT 309WAQTCT 359AASHTOPavement Thickness by Magnetic Pulse InductionC 457ASTMMicroscopical Determination of Parameters of the Air-Void System inHardened ConcreteC 495ASTMCompressive Strength of Lightweight Insulated ConcreteT 716WSDOTT 802WSDOTWSDOT Materials ManualMay 2021üüFOP for WAQTC TM 2, Sampling Freshly Mixed ConcreteCompressive Strength of Cylindrical Concrete SpecimensüüFOP for AASHTO T 22, Compressive Strength of CylindricalConcrete SpecimensMaking and Curing Concrete Test Specimens in the FieldüüüüFOP for AASHTO T 23, Making and Curing Concrete Test Specimensin the FieldFOP for AASHTO for Compressive Strength of Hydraulic Cement Mortars(Using 2-in. or (50-mm) Cube Specimens)Slump of Hydraulic Cement ConcreteüüFOP for AASHTO T 119, Slump of Hydraulic Cement ConcreteDensity (Unit Weight), Yield, and Air Content (Gravimetric) of ConcreteüüüüüüüFOP for AASHTO T 121, Density (Unit Weight), Yield, and Air Content(Gravimetric) of ConcreteüFOP for AASHTO T 152, Air Content of Freshly Mixed Concrete by thePressure MethodüAir Content of Freshly Mixed Concrete by the Volumetric Method(Checklist Only)üüüüM 46-01.39FOP for AASHTO T 231, Capping Cylindrical Concrete SpecimensFOP for AASHTO T 309, Temperature of Freshly Mixed PortlandCement ConcreteMethod of Random Sampling for Locations of Testing and Sampling SitesMethod of Test for Flexural Strength of Concrete (Using Simple Beam WithCenter-Point Loading)P

M 251 AASHTO Plain and Laminated Elastomeric Bridge Bearings T 65 AASHTO Mass (Weight) of Coating on Iron and Steel Articles With Zinc or Zinc-Alloy Coatings T 105/ C114 AASHTO Chemical Analysis of Hydraulic Cement T 260 AASHTO Sampling and Testing for Chloride Ion in Concrete and Concrete Raw Materials T 267 AASHTO Determination of Organic Content in Soils by Loss on