Transcription
PITTCON Conferenceand Expo 2010AbstractsOrlando, Florida, USA28 February - 5 March 2010IndexISBN: 978-1-63439-018-74/4
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Technical ProgramSUNDAY, FEBRUARY 28, 2010AFTERNOONAWARDSession 10Pittcon Heritage Award and Plenary SpeakerSunday Afternoon, Room W320, Chapin Theater4:30Presentation of the 2010 Pittcon Heritage Award to Walter G Jennings, Universityof California at Davis, by Annette S Wilson, 2010 Pittcon PresidentImmediately followed by Plenary Lecture - Alan G Marshall, Florida State University - The Role of High-EndInstrumentationSYMPOSIUMSession 20ACS Division of Analytical Chemistry New Frontiers in Mass Spectrometric Analysis of Proteins- arranged by Heather Desaire, Kansas UniversitySunday Afternoon, Room 300Heather Desaire, Kansas University, Presiding1:00Introductory Remarks - Heather Desaire1:05(20-1)Structural Characterization of Pre-Amyloid Protein Oligomers Using CovalentLabeling and Mass Spectrometry RICHARD W VACHET, University of Massachusetts,Amherst, Vanessa L Mendoza, Shaynah Browne1:40(20-2)Developing Mass Spectrometry-based Tools for Biomarker Discovery inNeurodegenerative Diseases LINGJUN LI, University of Wisconsin, Xin Wei, RobertCunningham, Paige Jany, Feng Xiang, Allen Herbst, Albee Messing, Judd Aiken2:15(20-3)High-Throughput Pipeline for Discovery-to-Targeted Analysis of Topology andFunction in Integral Membrane Proteins CHRISTINE C WU, University of ColoradoSchool of Medicine2:50(20-4)Understanding and Controlling Gas-phase Ion Chemistry to Improve the AnalyticalCapabilities of Biological Mass Spectrometry for Phosphoproteome Analysis GAVINE REID, Michigan State University3:25(20-5)Emerging Strategies for Facilitating Glycoprotein Analysis HEATHER DESAIRE,University of Kansas
SYMPOSIUMSession 30Advances in Hand-portable Ion Mobility and Ion Trap Chemical Analyzers - arranged by Milton LLee, Brigham Young University and Herbert H Hill, Washington State UniversitySunday Afternoon, Room 311AMilton L Lee, Brigham Young University, Presiding1:00Introductory Remarks - Milton L Lee1:05(30-1)Microfabricated Planar Electrode Ion Traps: Combining Accuracy with Simplicityfor Miniaturization DANIEL E AUSTIN, Brigham Young University1:40(30-2)Ion Preparation before Differential Mobility Spectrometry (DMS) IncludingDMS/DMS Analyzers GARY ALAN EICEMAN, New Mexico State University2:15(30-3)Quantitative Detection in the Field Using Hand-portable GC-MS EDGAR D LEE,Torion Technologies Inc., Milton L Lee, Douglas W Later, Joseph L Oliphant, Carmela RJackson LePage, Philip A Smith, Charles S Sadowski, Tiffany C Wirth2:50(30-4)Portable Mass Spectrometers vs. Portable Mass Spectrometry AnalysisLaboratories ZHENG OUYANG, Purdue University,R Graham Cooks, He Wang, Jiangjiang Liu, Nicolas E Manicke, Guangming Huang3:25(30-5)Multidimensional Ion Mobility Spectrometer for High Fidelity ChemicalIdentification HERBERT H HILL, Washington State UniversitySYMPOSIUMSession 40Analytical Chemistry for the Study of Nanotoxicity - arranged by Wenwan Zhong, University ofCalifornia, RiversideSunday Afternoon, Room 206AWenwan Zhong, University of California, Riverside, Presiding1:001:05Introductory Remarks - Wenwan Zhong(40-1)A Role for Particle Surface Effects in TiO 2 and Quartz-related NanoparticlePulmonary ToxicityDAVID B WARHEIT, DuPont Haskell Global Centers1:40(40-2)Systems-Level Approaches to Understanding Nanoparticle Biocompatibility BRIAND THRALL, Pacific Northwest National Laboratory2:15(40-3)Nanoparticle-plasma Interactions: A Basis for Nanosafety Assessment KENNETHADRIAN DAWSON, University College Dublin2:50(40-4)The Study of Protein-nanomaterial Interaction with Free-solution SeparationTechniques WENWAN ZHONG, University of California, Riverside, Ni Li, Lei Ren
3:25(40-5)Gold Nanorod Uptake by Cultured Cells and the Mechanisms of Cytotoxicity at HighDoses CATHERINE J MURPHY, University of IllinoisSYMPOSIUMSession 50Emerging Materials in Separation Science - arranged by Matthew R Linford, Brigham Young Universityand Abdul Malik, University of South FloridaSunday Afternoon, Room 311BMatthew R Linford, Brigham Young University, Presiding1:00Introductory Remarks - Matthew R Linford1:05(50-1)Hyper-crosslinked Silica Phases: Emerging Materials in Separation Science PETERW CARR, University of Minnesota, Yu Zhang, Lianjia Ma, Hao Luo1:40(50-2)Titania- and Germania-based Hybrid Organic-Inorganic Sol-Gel Coatings andMonolithic Beds for Ultrahigh Stability in Separation Science ABDUL MALIK,University of South Florida, Scott S Segro, Erica B Turner, Minhphuong Tran, ChemgliangJiang, Abdullah Alhendal2:15(50-3)Porous Graphitic Carbon: A Solution for Difficult LC Separations HARALD RITCHIE,Thermo Fisher Scientific2:50(50-4)Functionalized Diamond as a Stationary Phase in Chromatography MATTHEW RLINFORD, Brigham Young University, Li Yang, Gaurav Saini, Wiest Landon, David SJensen, Andrew Dadson, Michael A Vail3:25(50-5)Micro and Nanofabrication of Chromatography Media ROBERT C DAVIS, BrighamYoung University, Vanfleet R Richard , Matthew R LinfordSYMPOSIUMSession 60Sol-Gel Materials for Chemical Analysis - arranged by Maryanne M Collinson, Virginia CommonwealthUniversitySunday Afternoon, Room 205BMaryanne M Collinson, Virginia Commonwealth University, Presiding1:00Introductory Remarks - Maryanne M Collinson1:05(60-1)High Surface Area Materials for Chemical Analysis MARYANNE M COLLINSON, VirginiaCommonwealth University1:40(60-2)Sol-Gel-Derived Mesoporous Silica Materials in Electroanalysis ALAIN WALCARIUS,LCPME-CNRS2:15(60-3)Sol-Gel Derived Thin Films for Spectroelectrochemical Sensors WILLIAM RHEINEMAN, University of Cincinnati, Carol J Seliskar, John A Lynch, Ronnee N Andrews
2:50(60-4)Nanocrystallite-xerogel Hybrids for Optical Sensing FRANK V BRIGHT, University atBuffalo, SUNY3:25(60-5)Sepsis Monitoring via Sol-Gel Derived Chemical Sensors MARK H SCHOENFISCH,University of North Carolina, Chapel Hill, Benjamin J PrivettSYMPOSIUMSession 70Ultrasmall and Ultrasensitive Chemical Imaging of Cells and Cell Networks "WEBCAST"arranged by Andrew G Ewing, Penn State UniversitySunday Afternoon, Room 205CAndrew G Ewing, Penn State University, PresidingIntroductory Remarks - Andrew G Ewing1:001:05(70-1)Probing Transport of Catecholamines in the Adrenal Gland with MicroelectrodesMARK WIGHTMAN, University of North Carolina, Chapel Hill1:40(70-2)Nanopore-based Artificial Ion-Channel Sensors for Monitoring Cell SecretionZHANG, University of Washington, Jin Chen2:15(70-3)Optodes: A New Approach to Imaging Chemicals at Single Cells in a NetworkANDREW G EWING, Penn State University/University of Gothenburg, Niklas Strömberg,Maja Puchades2:50(70-4)Tip-Enhanced Raman Spectroscopy Bio-spectroscopy Below 20-NanometerResolution VOLKER DECKERT, IPHT3:25(70-5)Mass Spectrometric Profiling and Imaging Approaches for Understanding theNeuronal Metabolome JONATHAN V SWEEDLER, University of IllinoisWORKSHOPBOSession 80Analytical Challenges Facing the U.S. Department of Energy Office of EnvironmentalManagement - arranged by Jacob Venzie, Savannah River National LaboratorySunday Afternoon, Room 311DJacob Venzie, Savannah River National Laboratory, PresidingIntroductory Remarks - Jacob Venzie1:001:05(80-1)An Overview of DOE-EM Technology and Engineering SHARON MARRA, SavannahRiver National Laboratory1:40(80-2)Analytical Methods for Monitoring Vitrification of Hanford Radioactive WasteARUNA V ARAKALI, URS-Washington Division, Kenneth R Wells, Thomas A Lane, Jinesh CJain, Douglas M Perkins2:15Recess
2:30(80-3)Analytical Challenges in the Department of Energy (DOE) Deactivation andDecommissioning Program JOHN GLADDEN, Savannah River National Laboratory,Andrew Szilagyi3:05(80-4)Unique Requirements for Analytical Tools in the EM Complex JACOB VENZIE,Savannah River National Laboratory3:40Discussion/Wrap UpORGANIZED CONTRIBUTED SESSIONSession 90SEAC Organized Session - Electrochemistry and Materials - arranged by Richard A Durst, CornellUniversitySunday Afternoon, Room 311CAnna Brajter-Toth, University of Florida, Presiding1:00(90-1)Treating Carbon Nanotube Arrays to Increase the Oxygen Species for FurtherFunctionalization AMOS DOEPKE, University of Cincinnati, Changseok Han, William RHeineman1:20(90-2)Scanning Electrochemical Microscopy of Individual Single-Walled CarbonNanotubes JIYEON KIM, University of Pittsburgh, Shigeru Amemiya1:40(90-3)Fourier Transform Voltammetry at Microelectrodes: Principles and ApplicationsANNA BRAJTER-TOTH, University of Florida, Alan M Bond, Darrell Elton, Chong-Yong Lee2:00(90-4)Investigating Surface Transformations Induced by Electrochemical Pretreatmentat Carbon Fiber Microelectrodes JAMES G ROBERTS, North Carolina State University,Benjamin P Moody, Greg S McCarty, Leslie Sombers2:20Recess2:35(90-5)Potential Application of Conducting Polymer Modified Electrodes for NeurologicalStimulation and Sensing ANTHONY KAMMERICH, Georgetown University, CameronSweeney, Patrick Forcelli, Karen Gale, Judith F Rubinson2:55(90-6)Carbon Fiber Microelectrode Coatings for Long-term Stability and Accuracy in Invivo Voltammetry YOGESH S SINGH, Penn State University, Lauren E Sawarynski,Anne M Andrews3:15(90-7)Electrochemical Analysis of Altered Degranulation Function of Mast Cells Exposedto Noble Metal Nanomaterials with Varied Physical Properties BRYCE J MARQUIS,University of Minnesota, Christy L Haynes, Zhen Liu3:35(90-8)Development and Characterization of Highly Efficient IntegratedBioelectrocatalytic Systems PAWEL J KULESZA, University of Warsaw, BarbaraKowalewska
ORAL SESSIONSession 100Art/Archaeology: Applications of Instrumental Analysis (Half Session)Sunday Afternoon, Room 310AKimberley Frederick, Skidmore College, Presiding1:00(100-1)Chemistry and Art: Interactions and Mutual Influence BRUNO BRUNETTI, Universityof Perugia1:20(100-2)Non-destructive Sample Preparation for Radiocarbon Dating of Textiles and OtherPerishable Archaeological Materials RUTH ANN ARMITAGE, Eastern MichiganUniversityORAL SESSIONSession 110Cells on ChipsSunday Afternoon, Room 307DGary L Emmert, The University of Memphis, Presiding1:00(110-1)Microfluidic Cell Culture with Dissolved Gas Control SAMUEL P FORRY, NIST, Peter CThomas, Laurie Locascio1:20(110-2)Microfluidic Platform for Algal Growth and Analysis RYAN E HOLCOMB, ColoradoState University, Lucas J Mason, Kenneth F Reardon, Charles S Henry1:40(110-3)Simultaneous Cell Capture and Induction of Apoptosis Using an Anti-CD95 AffinityMicrodevice RANDALL D REIF, Texas Tech University, Kelong Wang, Michelle M Martinez,Dimitri Pappas2:00(110-4)A Lab-on-a-Chip for Live Cell Analysis of Mammalian Cells Under Natural FluidFlow Conditions VERENA CHARWAT, Austrian Institute of Technology GmbH, Lukas ARichter, Peter Ertl, Johannes Grillari, Regina Grillari2:20Recess2:35(110-5)Multi-analyte Concentration Profiles Independently-controlled in a MicrofluidicDevice LIAORAN CAO, Florida State University, Michael G Roper2:55(110-6)Development of a Disposable Microfluidic Biochip for Multi-Parameter CellPopulation Measurements LUKAS A RICHTER, Austrian Institute of Technology, JohannaGottschamel, Andy Mak, Christian Jungreuthmayer, Gerald M Birnbaumer , Marcus Milnera,Hubert Brueckl, Peter Ert3:15(110-7)Living Cell Arrays Characterizing Macromolecular Complexes from TranscriptionalActivators JASON SHEPARD, University at Albany, SUNY, Hua Shi, Maureen Walling,Shengchun Wang3:35(110-8)Ultra-Sensitive Portable Capillary Whole-cell Biosensor for Cell Viability MonitoringQIONG WANG, SUNY-Binghamton, Omowunmi A Sadik, Paul A Blythe, Janet Tuan
ORAL SESSIONSession 120Characterization of Advanced Materials for Energy Generation (Half Session)Sunday Afternoon, Room 307BSingh Manocha, The Pittsburgh Conference, Presiding1:00(120-1)Withdrawn1:20(120-2)In situ Growth of Au Nanorods on TiO 2 Surfaces for Photoelectrochemical SolarCells AIZE LI, University of North Dakota, Nenny Fahruddin, David T Pierce, Julia X Zhao1:40(120-3)Performance Comparison of Enzymatic Biofuel Cells Using Graphene Nanosheetsand Carbon Nanotube Materials CHANG LIU, Florida International University, SubbiahAlwarappan, Chenzhong Li2:00(120-4)High Temperature Characterization of Ceramic SOFC Oxygen PermeationMembranes ROBERT JOHN PACKER, PerkinElmer, Kevin P Menard, Peng Ye, SarahTheelanORAL SESSIONSession 130Chemical Methods (Half Session)Sunday Afternoon, Room 307AMark T Stauffer, University of Pittsburgh at Greensburg, Presiding2:35(130-1)The Anatomy of Commercial Tricalcium Phosphates BOBBY LATHAN SR., HydriteChemical Co.2:55(130-2)Improved SDS Concentration Determination Method KEVIN R RUPPRECHT, AbbottLaboratories, Tracey Rae, Troy D McSherry, Mary K Poterek, Ewa Lang, Jeffrey Fishpaugh3:15(130-3)Development of Novel Functional DNA Using Artificial Photoresponsive BasesRUOWEN WANG, University of Florida, Hui Wang, Huaizhi Kang, Haipeng Liu, WeihongTan3:35(130-4)Use of Polylysine as a Carrier for Signal Amplification in DNA Detection HONGQIAN, North Carolina State University, Lin HeORAL SESSIONSession 140ChemometricsSunday Afternoon, Room 205AKatherine A Bakeev, CAMO Software, Inc., Presiding1:00(140-1)Batch Monitoring of Pharmaceutical Processes with End-point Detection ModelsKATHERINE A BAKEEV, CAMO Software, Frank Westad
1:20(140-2)Optimization of Calibration Database Structure in Near Infrared SpectroscopyThrough the use of PLS1 Score Matrix PAOLO BERZAGHI, University of Padua - Italy,John S Shenk, John W Shenk8:40(140-3)Further Developments in K-matrix Calibration HOWARD MARK, Mark 5)Kernel-Based One-Class Nearest Neighbor Approach for Identification ofChlorinated Solvents MICHAEL G MADDEN, Analyze IQ, Shehroz S Khan2:55(140-6)Adaptive Polynomial Approximation of Chromatographic Peaks YURI KALAMBET,Ampersand International, Inc., Yuri Kozmin, Sergey Maltsev, Dmitry Gladkov3:15(140-7)Comparison of Feature Selection Techniques for Chemometric Analysis of GC-MSData NIKOLAI A SINKOV, University of Alberta, James J Harynuk3:35(140-8)An Automated Kiwifruit Harvest Estimation System: A Computer Vision BasedApproach PAVITHRA A WIJETHUNGA, Lincoln University, Sandhya Samarasinghe, DonKulasiri, Ian WoodheadORAL SESSIONSession 150Drug Discovery (Half Session)Sunday Afternoon, Room 307AMark T Stauffer, University of Pittsburgh at Greensburg, Presiding1:00(150-1)In Preparative Scale Gradient Reversed-phase Liquid Chromatography, Loadability and Peak Shape as a Function of pH and Buffer Concentration for BasicCompounds are Readily Rationalized Based on the Interaction of Eluent Conditionswith Analyte Properties MARK J HAYWARD, Lundbeck, Xu Zhang1:20(150-2)Use of an Integrated Ceramic Micro Fluidic Device for the Qualitative andQuantitative Analysis of Drugs and Metabolites in Biological Fluids ROBERT SPLUMB, Imperial College, Paul Rainville1:40(150-3)Direct Comparison of HPLC and SFC for the Milligram to Gram Scale Purification ofEnantiomers PETER RAHN, Phenomenex, Irene Tranquil, Gary Yanik2:00(150-4)Assessing Biology Through Coupling of Active Ingredients: Theoretical andSynthetic Approach Towards the Biology of Some Novel Monobactam InducedSulphonamides JYOTSNA SUDHIR MESHRAM, Nagpur University, Parvez AliORAL SESSIONElectrochemistrySession 160
Sunday Afternoon, Room 308ARose Clark, Saint Francis University, Presiding1:00(160-1)Development of Catalytic Adsorptive Stripping Voltammetric Methods for theDetermination of Ultra-trace Cr and V ROYCE N DANSBY-SPARKS, University ofTennessee, Ilia N Ivanov, Clarissa E Tatum, Stefanie A Bragg, Ruizhuo Ouyang, James QChambers, Zi-ling Xue1:20(160-2)Multifunctional Electrocatalysts Based on Combination of Transition-MetalSubstituted Polyoxometalates with Gold Nanoparticles KAMILA M WIADEREK , MiamiUniversity, Ohio, James A Cox1:40(160-3)Porphyrins Modified with Crown-ether Functionalities as Hyphenated Ionophoresfor Solvent Polymeric Membrane Electrodes LARISA LVOVA, University of Rome "TorVergata", Giuseppe Pomarico, Roberto Paolesse, Corrado Di Natale, Arnaldo D'Amico,Olga Mednova, Dmitry Kirsanov, Andrey Legin, Yuri G Vlasov2:00(160-4)Non-Nerstian Behavior of Anion-Selective Electrodes Prepared from PhosphoniumIonic Liquids R DANIEL JOHNSON, Murray State University, Rajani Gourishetty, Ann MCrabtree2:20Recess2:35(160-5)Histamine-pH Microelectrode Array to Understand Spatial Variations in GastricAcid Release from Isolated Stomach Tissue ELENI BITZIOU, Imperial College London,Danny O'Hare, Bhavik A Patel2:55(160-6)Electrochemistry in an Acoustically Levitated Drop EDWARD CHAINANI, University ofIllinois, Urbana-Champaign, Zakiah N Pierre, Steven M Markwell, Alexander Scheeline3:15(160-7)Enzyme-Amplified Electrochemical Detection of Whole Viral Particles BRYCE DAVIS,University of California, Riverside, Harry Lee, Quan Cheng3:35(160-8)Preparation of Chromium Sulfide Nanoparticles and Their Application as Cr(III)selective Electrode GAURANG M PATEL, Gujarat University, Shobhana MenonORAL SESSIONSession 170Food Science - Elemental AnalysesSunday Afternoon, Room 308BRobert W Baudoux, RWB Convention Mgt, Presiding1:00(170-1)The Analysis of Trace Elements in Rice Products Using Affordable and AccurateAtomic Absorption Spectroscopy MARTIN J NASH, Thermo Fisher Scientific, RebeccaPrice, Hazel Dickson1:20(170-2)Total Sulfur in Wine Using a Combustion Analyzer with UV-Fluorescence DetectionGUIDO GIAZZI, Thermo Fisher Scientific, Liliana Krotz, Martin J Nash, Ben Tordoff, FergusKeenan, Debbie Batt
1:40(170-3)Determination of Total and Hexavalent Chromium in Commercially AvailableChromium Supplements by Speciated Isotope Dilution Mass Spectrometry (EPAMethod 6800) Using IC-ICP-MS G M MIZANUR RAHMAN, Duquesne University, HowardM Kingston, Timothy Fahrenholz, Naudia Martone, Matt Pamuku, William Obermeyer,Amanda Anderson2:00(170-4)Trace Elemental Characterization of Edible Oils with Graphite Furnace AtomicAbsorption Spectrophotometer PRAVEEN SAROJAM, PerkinElmer Analytical Sciences,Zoe Grosser, Anil Nimkar2:20Recess2:35(170-5)Sulfur Speciation Analysis by Ion-Chromatography Hyphenated to InductivelyCoupled Plasma Mass Spectrometry ZHONGWEN WANG, Food Research Division,Health Canada, Melissa Sparling, Don Forsyth2:55(170-6)Determination of Iodide and Iodate in Saline Matrices by Anion ExchangeChromatography and HPLC DEANNA C HURUM, Dionex Corporation, Brian M De Borba,Jeffrey S Rohrer3:15(170-7)Nitrogen/ Protein Determination in Food Using Large Sample Weight by FlashCombustion as Alternative to Kjeldahl Method LILIANA KROTZ, Thermo FisherScientific, Guido Giazzi3:35(170-8)Optimization of Nitrogen Determination in Dietary Fiber (Celite) Analysis byCombustion Method AN SLEGERS, Laboratorium Ecca NV, Liliana Krotz, Roel Wuyts,Jean-Louis Brix, Guido GiazziORAL SESSIONSession 180GC DetectorsSunday Afternoon, Room 308CSteven B Dorn, Momentive Performance Materials, Presiding1:00(180-1)Dual Discharge Photo Ionization Detector for Gas ChromatographyVICI Valco Instruments Co. Inc., Stanley D Stearns1:20(180-2)Characterization of Non-radioactive Electron Capture Detector Based on theDielectric Barrier Discharge Plasma MATTHEW MONAGLE, AIC Corporation1:40(180-3)Low-volume Pulsed Discharge Electron Capture Detector STANLEY D STEARNS, VICIValco Instruments Co. Inc., Huamin Cai, Alex Plistil2:00(180-4)A Planar Micro Flame Ionization Detector for 2D Micro Gas ChromatographyWINFRED JAN KUIPERS, Hamburg University of Technology, Joerg Mueller2:202:35HUAMIN CAI,Recess(180-5)A New PID for Trace Analysis JOHN N DRISCOLL, PID Analyzers, LLC, George Sprague
ORAL SESSIONSession 190GC Sample Introduction/New Columns/OptimizationSunday Afternoon, Room 207CWilliam E Barber, Agilent Technologies, Inc., Presiding1:00(190-1)Innovations in Valve Technology – Low Level Analysis – from the Lab Bench to theProcess Analyzer GORDON MCFARLANE, Analytical Flow Products, Yves Gamache1:20(190-2)The Use of Thermal Desorption for a Range of Consumer Safety Concerns!STEPHEN D WESSON, CDS Analytical, Thomas Wampler, Karen Jansson1:40(190-3)Form and Function: Understanding the Complex World of Gas ChromatographicInlet Liners SCOTT LANDER GROSSMAN, Restek Corporation, Corby Hilliard, JackCochran2:00(190-4)Adaptation of Monolithic High Performance Liquid Chromatography Columns forGas Chromatographic Separation Prior to Ion Mobility Spectrometry LINDA JONES,Sandia Staffing Alliance, Peter Hotchkiss, James Spates, David A Jones2:20Recess2:35(190-5)Effect of Carrier Gas Upon the Determination of Thermodynamic Parameters Usedto Predict Retention Time in Gas Chromatography JAMES J HARYNUK, University ofAlberta, Teague McGinitie2:55(190-6)Polar and Highly Polar Ionic Liquid Capillary Columns LEONARD SIDISKY,Supleco/Sigma-Aldrich, Yizeng Ni, Greg A Baney, James L Desorcie, Katherine Stenerson3:15(190-7)Preparative Purification of Expressed Proteins by Spiral CountercurrentChromatography MARTHA KNIGHT, CC Biotech LLC, Aprile Pilon, Thomas M FinnORAL SESSIONSession 200High Throughput Chemical AnalysisSunday Afternoon, Room 308DEmelita Breyer, Emory University, Presiding1:00(200-1)Particle Imaging of Powder Samples as a Pre-screen Tool to Detect and QuantifyMicrobial Contamination JANIE DUBOIS, Malvern Instruments, Kenneth Haber, Linda HKidder, E Neil Lewis1:20(200-2)Micro Scale Synthesis of ILs: A Novel Approach Using a Digital Microfluidic ChipYASITH S NANAYAKKARA, The University of Texas at Arlington, Praveen Kunchala, HyejinMoon, Daniel Armstrong1:40(200-3)Applications of New Silica-Based SPE Cartridges DAVID E KNOWLES, Dionex, Eric SFrancis, Richard E Carlson, Brian C Dorich, Kannan Srinivasan, SM Rahmat Ullah, BruceRichter
2:00(200-4)2:20Parallel Screening/Separation Method Development by Supercritical FluidChromatography ZIQIANG WANG, TharSFC, Harbaksh Sidhu, Michael WebsterRecess2:35(200-5)On-chip Liquid-liquid Extraction and Separation Using Digital Microfluidics TowardHigh-throughput Screening for Separation Process Using Ionic Liquids HYEJINMOON, University of Texas at Arlington, Praveen Kunchala, Yasith S Nanayakkara, DanielArmstrong2:55(200-6)Improving Analyte Stream Stability in Micro-Free Flow Electrophoresis by Additionof Surfactant and Use of Mixed Aqueous/Nonaqueous Carrier Buffers NICHOLAS WFROST, University of Minnesota, Michael T BowserORAL SESSIONSession 210Microscopy: New Instrumental TechniquesSunday Afternoon, Room 206BYinfa Ma, Missouri University of Science and Technology, Presiding1:00(210-1)Investigations of Translational and Rotational Motions in Living Cells UsingPlasmonic Nanoprobes and Differential Interference Contrast Microscopy NINGFANG, Iowa State University, Gufeng Wang, Wei Sun1:20(210-2)Using Laser-Scatter Triggering in an Imaging Particle Analysis System to IncreaseParticle Counting Accuracy in Sparse Samples LEW BROWN, Fluid ImagingTechnologies, Inc.1:40(210-3)A High Throughput Surface Plasmon Based Image Filter for Wide-field ChemicalImaging NICK PALLAS, Cleveland State University, John F Turner2:00(210-4)Advances in Automated Chemical Imaging JOHN F TURNER, Cleveland StateUniversity, Nikolas J Neric, Anita Wiederholt2:20Recess2:35(210-5)Correlative Microscopy: Concurrent SEM and Optical Imaging of Materials in TheirNative State DONNA GUARRERA, JEOL USA, Inc., Mitsuo Suga, Hidetoshi Nishiyama2:55(210-6)ATR Objectives for FT-IR Microscopy – The Advantages of ATR Imaging for MicroSample Analysis RICHARD A LARSEN, Jasco, Inc., John Carriker, Ken-ichi Akao, MiyukiShimomura, Jun Koshoubu, Toshiyuki Nagoshi3:15(210-7)Characterization of Nanomaterials Using Advanced FESEM/STEM and XPSTechniques BRIAN R STROHMEIER, RJ Lee Group, Inc., John D Piasecki, Kristin LBunker, Jacqueline L Sturgeon, James P Marquis, Traci L Lersch, Keith Wagner3:35(210-8)Real-time Imaging of Transport and Diffusion of Single Gold Nanoparticles In VivoLAUREN BROWNING, Old Dominion University, Kerry J Lee, Prakash D Nallathamby, TaoHuang, Jill Lowman, X Nancy Xu
ORAL SESSIONSession 220Neurochemistry ISunday Afternoon, Room 309ABParastoo Hashemi, University of North Carolina, Chapel Hill, Presiding1:00(220-1)Selective Glutamate Biosensor Arrays Integrated on Silicon Microprobes for In vivoBrain Recordings OLIVIER FREY, EPF Lausanne, Ruth McNamara, Jefferey W Dalley,Peter D van der Wal, Nico F de Rooij, Trevor W Robbins, Milena Koudelka-Hep1:20(220-2)Robust Pyrolyzed Photoresist Microelectrodes for Voltammetric Detection ofCatecholamines In vitro and In vivo PAVEL TAKMAKOV, University of North Carolina,Chapel Hill, Richard B Keithley, Paul L Walsh, Natalie R Herr, Jinwoo Park, Matthew KZachek, Mark Wightman1:40(220-3)Electrochemical Methods to Measure the Total Neurotransmitter Content inVesicles LISA JOSEFINA MELLANDER, Gothenburg University, Donna M Omiatek, AndrewG Ewing2:00(220-4)Towards Understanding Ultrastructural Tissue Differences Associated with Rapidand Slow Signaling of Dopamine ANDREA JAQUINS-GERSTL, University of Pittsburgh,Adrian C Michael2:20Recess2:35(220-5)Improving Principal Component Regression Analysis of Fast-scan CyclicVoltammetric Data RICHARD B KEITHLEY, The University of North Carolina, Regina MCarelli, Mark Wightman2:55(220-6)Electrochemical Monitoring of Norepinephrine and Dopamine Overflow in the BedNucleus of the Stria Terminalis of Freely Moving Rats JINWOO PARK, University ofNorth Carolina, Khristy Fontillas, Mark Wightman3:15(220-7)An Electrochemical Study of The Role of Membrane Cholesterol in ExocytosisSHENCHENG GE, University of Minnesota, James G White, Christy L Haynes3:35(220-8)Carbon Based Arrays for In vivo Detection of Catecholamines MATTHEW K ZACHEK,University of North Carolina, Pavel Takmakov, Mark Wightman, Greg S McCartyORAL SESSIONSession 230Novel Sensor TechnologiesSunday Afternoon, Room 207BWilliam R LaCourse, University of Maryland, Baltimore County, Presiding1:00(230-1)Enhanced Gas Sensing of SnO2 Functionalized SWNTs by Catalyst NanoparticleImpregnation – A Repeated Electrochemical Templating Approach SYED MUBEEN
JAWAHAR HUSSAINI, University of California, Riverside, Marc A Deshusses, AshokMulchandani, Nosang V Myunh1:20(230-2)Detection of Environmental Contaminants Using Nanotechnology RESHMI SBANERJEE, Florida International University, Chenzhong Li1:40(230-3)Gas Analyzer for Continuous Monitoring of Sulfur Dioxide in Gas Streams Based onAmperometric Detector SAYED MARZOUK, UAE University, Mohamed Al Marzouqi2:00(230-4)SPR Biosensors Protected by Near-zero Fouling Peptide Monolayers to DetectBiomolecules in Complex Biofluids JEAN-FRANCOIS MASSON, Universite de Montreal,Olivier Bolduc, Christopher Clouthier, Joelle Pelletier2:20Recess2:35(230-5)Transport Behavior of Perfluorotripentylamine (FC-70)-doped Teflon AF 2400Membranes HONG ZHANG, University of Pittsburgh, Stephen G Weber, Abul Hussam2:55(230-6)MEMS Micro-pirani Sensor and Reading Method for Pressure Measurements inSmall Volumes with Low Temperature Dependence MARCO MICHELE SISTO, INO,Sonia Garcia Blanco, Loic Le Noc, Yan Desroches, Francis Provencal, Jean-Sol Caron,Francis Picard, Patrice Topart3:15(230-7)MEMS Grating Based Micro-spectrometers and Tunable Lasers for Visible, Nearand Mid-Infrared Applications MAURIZIO TORMEN, CSEM, Robert Lockhart, BranislavTimotijevic , Thomas Overstolz, Ross Stanley, Jorg Pierer, Real Ischer, Guy Voirin3:35(230-8)Development of Surface-immobilized Aptasensors for Small Molecule and ProteinDetection TAO CHEN, University of FloridaORAL SESSIONSession 240Pharmaceutical Problem SolvingSunday Afternoon, Room 310BBruce P McPherson, Meda Pharmaceuticals, Presiding1:00(240-1)Use of Process Measurement Technology in the Development/Scale-Up of RollerCompaction Processes ZANE ALLEN ARP, GlaxoSmithKline, Tamika Hayden, BrianRhodes, Alfonzo Taggart1:20(240-2)Biorelevant Dissolution Testing KEVIN C BYNUM, Boehringer IngelheimPharmaceuticals, Inc., Stephen Cafiero, Henry Zhao1:40(240-3)Visual Observations During Dissolution Testing STEPHEN CAFIERO, BoehringerIngelheim Pharmaceuticals, Inc., Kevin C Bynum2:00(240-4)Identifying Phase Transformations of a Pharmaceutical Co-Crystal on StabilityLISA DELATTRE, Boehringer Ingelheim Pharmaceuticals, Inc., Karen Weigandt, Kevin CBynum, James Murner, Thomas Offerdahl, John Smoliga, George Gereg, Pragati Reddy,Jung Park
2:20Recess2:35(240-5)Surface Enhanced Raman Spectroscopy as a Tool for Cleaning Verification in thePharmaceutical Industry DAVID ANDREW EUSTACE, D3 Technologies Ltd, GraemeMcNay, Kirstin A Lynn, Michael A Gallagher, Maria C Netti, William E Smith2:55(240-6)Effect of Alcohol on the Dissolution of an Extended Release Tablet BRUCE PMCPHERSON, Meda Pharmaceuticals, Charles W Stewart, Robert J Allara, Syed Hussain,Alexander D'Addio3:15(240-7)Rapid and Simple Headspace GC Method to Quantify Formic Acid and Acetic Acid inDrug Products HONG CHEN, Nexgen Pharma, Luis Vidaurrazaga, Ian Gibson, Bob vanOsdel3:35(240-8)Preparation of Acyclovir Loaded Niosomal Nano Vesicles Using Reverse PhaseEvaporation Technique AJAY PAL SINGH, Al-Arab Medical University, Ashok Kaushal,Wafa M Ramadan, Idrish MehdiORAL SESSIONSession 250Sensors for BioanalysisSunday Afternoon, Room 307CJoshua Smith, Armstrong Atlantic State University, Presiding1:00(250-1)Continuous Glucose Monitoring with an Ultrafi
ISBN: 978-1-63439-018-7 PITTCON Conference and Expo 2010 Orlando, Florida, US
