LABORATORY REPORT

Transcription

SDMS DOCID#11421974625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)454-9303LABORATORY REPORTPrepared For:AMEC Geomatrix Consultants, Inc. - AZ - PGAN8777 E. Via de Ventura, Suite 396Scottsdale, AZ 85258Attention: Mike DempseyProject: 08-227ESampled: 05/11/09Received: 05/11/09Issued: 05/22/09 09:45NELAP #01109CA Arizona DHS#AZ0728The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this reportwere performed in accordance with the applicable certifications as noted. All soil samples are reported on a wet weight basis unlessotherwise noted in the report. This Laboratory Report is confidential and is intended for the sole use of TestAmerica and its client. Thisreport shall not be reproduced, except in full, without written permission from TestAmerica. The Chain of Custody, 1 page, is included andis an integral part of this report.This entire report was reviewed and approved for release.CASE NARRATIVELABORATORY IDCLIENT IDMATRIXPSE0580-01Bd2-05112009WaterSAMPLE RECEIPT:Samples were received intact, at 3 C, on ice and with chain of custody documentation.HOLDING TIMES:All samples were analyzed within prescribed holding times and/or in accordance with the TestAmericaSample Acceptance Policy unless otherwise noted in the report.PRESERVATION:Samples requiring preservation were verified prior to sample analysis.QA/QC CRITERIA:All analyses met method criteria, except as noted in the report with data qualifiers.COMMENTS:No significant observations were made.SUBCONTRACTED:No analyses were subcontracted to an outside laboratory.Reviewed By:TestAmerica PhoenixTina PaulauskasProject ManagerPSE0580 Page 1 of 5

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)454-9303AMEC Geomatrix Consultants, Inc. - AZ - PGAN8777 E. Via de Ventura, Suite 396Scottsdale, AZ 85258Attention: Mike DempseyProject ID: 08-227ESampled: 05/11/09Received: 05/11/09Report Number: PSE0580TOTAL METALSAnalyteMethodBatchReportingLimitSample DilutionDateResult Factor ExtractedDateAnalyzedDataQualifiersSample ID: PSE0580-01 (Bd2-05112009 - Water)Reporting Units: 2009TestAmerica PhoenixTina PaulauskasProject ManagerThe results pertain only to the samples tested in the laboratory. This report shall not be reproduced,except in full, without written permission from TestAmerica.PSE0580 Page 2 of 5

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)454-9303AMEC Geomatrix Consultants, Inc. - AZ - PGAN8777 E. Via de Ventura, Suite 396Scottsdale, AZ 85258Attention: Mike DempseyProject ID: 08-227ESampled: 05/11/09Received: 05/11/09Report Number: PSE0580METHOD BLANK/QC DATATOTAL urceResult%REC%RECLimits RPDRPDLimitDataQualifiersBatch: P9E1132 Extracted: 05/11/09Blank Analyzed: 05/13/2009 /l0.500LCS Analyzed: 05/13/2009 (P9E1132-BS1)ChromiumLCS Dup Analyzed: 05/13/2009 (P9E1132-BSD1)Chromium0.515Matrix Spike Analyzed: 05/13/2009 (P9E1132-MS1)Chromium0.4860.48320110Source: PSE0547-03Matrix Spike Dup Analyzed: 05/13/2009 (P9E1132-MSD1)Chromium10.0100.004439675-125Source: PSE0547-030.004439675-125TestAmerica PhoenixTina PaulauskasProject ManagerThe results pertain only to the samples tested in the laboratory. This report shall not be reproduced,except in full, without written permission from TestAmerica.PSE0580 Page 3 of 5

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)454-9303AMEC Geomatrix Consultants, Inc. - AZ - PGAN8777 E. Via de Ventura, Suite 396Scottsdale, AZ 85258Attention: Mike DempseyProject ID: 08-227EReport Number: PSE0580Sampled: 05/11/09Received: 05/11/09DATA QUALIFIERS AND DEFINITIONSNDAnalyte NOT DETECTED at or above the reporting limit or MDL, if MDL is specified.RPDRelative Percent DifferenceTestAmerica PhoenixTina PaulauskasProject ManagerThe results pertain only to the samples tested in the laboratory. This report shall not be reproduced,except in full, without written permission from TestAmerica.PSE0580 Page 4 of 5

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)454-9303AMEC Geomatrix Consultants, Inc. - AZ - PGAN8777 E. Via de Ventura, Suite 396Scottsdale, AZ 85258Attention: Mike DempseyProject ID: 08-227EReport Number: PSE0580Sampled: 05/11/09Received: 05/11/09Certification SummaryTestAmerica PhoenixMethodMatrixE200.7WaterNelacArizonaXNevada and NELAP provide analyte specific accreditations. Analyte specific information for TestAmerica may be obtained by contactingthe laboratory or visiting our website at www.testamericainc.comTestAmerica PhoenixTina PaulauskasProject ManagerThe results pertain only to the samples tested in the laboratory. This report shall not be reproduced,except in full, without written permission from TestAmerica.PSE0580 Page 5 of 5

TestAmericaCHAIN OF CUSTODY FORM.f\i.Phoenix- 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ. 85040 (602) 437-3340 FAX (602) 454-9303[ ] Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803[ ] Las Vegas- 2520 E. Sunset, Suite 3, Las Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621'Project! PO Number:Analysis RequiredTHE LEADER IN ENVIRONMENTAL TESTINGTAL-0013·550 (12/08)Client t,me/AddressM;n,.z:.r;JtJ MvlM E& f/J .1/'e.e.i J'lr!& It /fve . .P utJt-)l? f»)lPageofJf/8'1Z858oj/J /J?t:JJir Project Manager: jh,:Ae. iJe.7'Je.JPhone Number:(1?3) {}. 'fCJSampler:Fax Number:j-tS{) () u; rt. Lawrt.-.t.tSam pi{ Description/ld :1- II :ltJIJ1 edBy: .4"/'" .y7I'Relinquisi! dRelinquished By:"' ·p --Sample· ContainerTypeMatrixlit){)#ofCont.'- /llllfQ@I?J) ). ytl- JJJ8SamplingDate, ptY l"&l't- Special instructions-X&s1 I '2.-r .1-e ve.21Date/Time:(r7eived By:Turnaround Time:)Lj}dDate/Time:Date/Time:f,t Tl 1()5/Jt/11 e/Time:Jfeceived By:(/17/l tJtJ Lab By:v. . III0;.Date/Time:ll '1/"-t o.(Check)same day72 hours24 hours5 days48 hoursnormalSample Integrity:intact/(Check)on iceNote: By rehnqUishmg samples to TestAmerrca, client agrees to pay for the serv1ces requested on th1s cham of custody form and any additiOnal analyses performed on this project.Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.J("a:: .3 .;.\ . 0

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)454-9303LABORATORY REPORTPrepared For:AMEC Geomatrix Consultants, Inc. - AZ - PGAN8777 E. Via de Ventura, Suite 396Scottsdale, AZ 85258Attention: Brian McnamaraProject: PGAN 14682.013Sampled: 07/15/09Received: 07/15/09Issued: 07/30/09 13:27NELAP #01109CA Arizona DHS#AZ0728The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this reportwere performed in accordance with the applicable certifications as noted. All soil samples are reported on a wet weight basis unlessotherwise noted in the report. This Laboratory Report is confidential and is intended for the sole use of TestAmerica and its client. Thisreport shall not be reproduced, except in full, without written permission from TestAmerica. The Chain of Custody, 1 page, is included andis an integral part of this report.This entire report was reviewed and approved for release.CASE NARRATIVELABORATORY IDCLIENT d 22-9-07152009Bld 22-10.1-07152009Bld 22-10.2-07152009Bld 22-10.1-07152009SoilOilSoilOilTestAmerica PhoenixTina PaulauskasProject ManagerPSG0914 Page 1 of 22

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)454-9303AMEC Geomatrix Consultants, Inc. - AZ - PGAN8777 E. Via de Ventura, Suite 396Scottsdale, AZ 85258Attention: Brian McnamaraProject ID: PGAN 14682.013Report Number: PSG0914Sampled: 07/15/09Received: 07/15/09SAMPLE RECEIPT:Samples were received intact, at 9 C, on ice and with chain of custody documentation.HOLDING TIMES:All samples were analyzed within prescribed holding times and/or in accordance with the TestAmericaSample Acceptance Policy unless otherwise noted in the report.PRESERVATION:Samples requiring preservation were verified prior to sample analysis.QA/QC CRITERIA:All analyses met method criteria, except as noted in the report with data qualifiers.L3-Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above theacceptance limits. Analyte not detected, data not impacted.N1a- Vinyl Acetate - The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).N1a- 2-Butanone - The LCS/LCSD and MSD recovered high and outside of acceptance limits for2-Butanone. All associated samples are non-detect for 2-Butanone and therefore should not be impacted.COMMENTS:No significant observations were made.SUBCONTRACTED:No analyses were subcontracted to an outside laboratory.Reviewed By:TestAmerica PhoenixTina PaulauskasProject ManagerThe results pertain only to the samples tested in the laboratory. This report shall not be reproduced,except in full, without written permission from TestAmerica.PSG0914 Page 2 of 22

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)454-9303AMEC Geomatrix Consultants, Inc. - AZ - PGAN8777 E. Via de Ventura, Suite 396Scottsdale, AZ 85258Attention: Brian McnamaraProject ID: PGAN 14682.013Sampled: 07/15/09Received: 07/15/09Report Number: PSG0914EXTRACTABLE FUEL HYDROCARBONS (EPA 3510/8015B)AnalyteMethodBatchReportingLimitSample DilutionDateResult Factor ExtractedDateAnalyzed810000 97.1320000 97.11100000 ple ID: PSG0914-04 (Bld 22-10.1-07152009 - Oil)Reporting Units: mg/kgDRO (C10-C22)ORO (C22-C32)Total (C10-C32)Surrogate: o-terphenyl (70-130%)EPA 8015DEPA 8015DEPA /21/20097/21/2009M3M3S8TestAmerica PhoenixTina PaulauskasProject ManagerThe results pertain only to the samples tested in the laboratory. This report shall not be reproduced,except in full, without written permission from TestAmerica.PSG0914 Page 3 of 22

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)454-9303AMEC Geomatrix Consultants, Inc. - AZ - PGAN8777 E. Via de Ventura, Suite 396Scottsdale, AZ 85258Attention: Brian McnamaraProject ID: PGAN 14682.013Sampled: 07/15/09Received: 07/15/09Report Number: PSG0914VOLATILE ORGANICS BY GC/MS (EPA 5035/8260B)AnalyteMethodBatchReportingLimitSample DilutionDateResult Factor ExtractedDateAnalyzedDataQualifiersSample ID: PSG0914-01 (Bld 22-9-07152009 - Soil)Reporting Units: romoethane ropropane2-Butanone hyl-2-pentanone BromodichloromethaneBromoformBromomethaneCarbon 97/16/2009L3L3L3TestAmerica PhoenixTina PaulauskasProject ManagerThe results pertain only to the samples tested in the laboratory. This report shall not be reproduced,except in full, without written permission from TestAmerica.PSG0914 Page 4 of 22

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)454-9303AMEC Geomatrix Consultants, Inc. - AZ - PGAN8777 E. Via de Ventura, Suite 396Scottsdale, AZ 85258Attention: Brian McnamaraProject ID: PGAN 14682.013Sampled: 07/15/09Received: 07/15/09Report Number: PSG0914VOLATILE ORGANICS BY GC/MS (EPA 5035/8260B)AnalyteMethodBatchReportingLimitSample DilutionDateResult Factor ExtractedDateAnalyzedDataQualifiersSample ID: PSG0914-01 (Bld 22-9-07152009 - Soil) - cont.Reporting Units: ug/kgm,p-XylenesMethyl-tert-butyl E

Analyte Method Date Extracted Date Analyzed Dilution Factor TOTAL METALS Data Batch Qualifiers Reporting Limit Sample Result Sample ID: PSE0580-01 (Bd2-05112009 - Water) Reporting Units: mg/l Chromium E200.7 P9E1132 0.010 0.029 1 5/11/2009 5/13/2009 Project Manager TestAmerica Phoenix PSE0580 Tina Paulauskas The results pertain only to the samples tested in the laboratory. This report