Distillation Chapter 5 - Specialty Glass, Inc

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DISTILLATION07-1000: DISTILLATION APPARATUS, CYANIDE - For use in determination ofcyanide in water in accordance with ASTM D2036Code #01020304050607DescriptionComplete as shownFlask 1000mlInlet tubeCold finger jacketCold fingerAbsorber tube with coarse fritted discAbsorber jacket07-1020: DISTILLING APPARATUS - Inverted Friedrich spiral condenser withholes in the top for vapors to exit. Connected to Erlenmeyer flask byjoint 500mlflask. Vapors are cooled and condensed descending the spiral and exit the sidearm.Code # 24/40 Description01Flask02Condenser03Complete07-1040: DISTILLING APPARATUS - Standard Friedrich Condenser connectedto Erlenmeyer flask byjoint. 5000ml flask.Code # 24/40010203DescriptionFlaskCondenserCompleteTo Order, Call Specialty Glass, Inc. Toll Free 1-800-899-213730

DISTILLATION07-1060: DISTILLATION APPARATUS - For general purpose distillations.Code 4024/4024/40DescriptionTrap1000ml Flask3000ml Flask5000ml Flask300mm Condenser400mm Condenser500mm CondenserConnecting Adapter07-1080: DISTILLATION APPARATUS - Solvent re-purification. For use indistillation, reflux, storage and dispensation of solvents. Double oblique Teflon stopcock allows for reflux, sample take-off, or storage of solvent. All joints are24/40 .Code #010203040506DescriptionDistilling head onlyBoiling flask with thermo -wellBoiling flask with thermo -wellBoiling flask with thermo -wellDispensing flaskDispensing flaskFlask Size1000ml2000ml3000ml500ml1000ml07-1100: DISTILLATION COLUMN, HEMPELL joints form the ends ofthis plain column. The bottom has small indentations for use as support forpacking material. Length of column is measured from the bottom of the top jointto the top of the indentions.Column Lengthmm300400500600900ID 12.5mm Code24/4001020304ID 19mm Code24/400506070809ID 25mm Code29/421011121314To Order, Call Specialty Glass, Inc. Toll Free 1-800-899-213731

DISTILLATION07-1120: DISTILLATION COLUMN, HEMPEL, VACUUM JACKETED – Thejacket allows the column to be used as a condenser. With indentations to supportpacking material.ColumnLength mm300400500600900ID 12.5mmCode 24/4001020304ID 19mmCode 24/400506070809ID 25mmCode 29/421011121314ID 19mmCode 35/25151617181907-1140: DIS TILLATION COLUMN, HEMPEL, VACUUM JACKETED,SILVERED - Same as 07-1120, except column is silvered.ColumnLength mm300400500600900ID 12.5mmCode 24/4001020304ID 19mmCode 24/400506070809ID 25mmCode 29/421011121314ID 19mmCode 35/25151617181907-1180: DISTILLATION COLUMN, VIGREUX - Vacuum jacketed Vigreuxstyle column with indentations that run the entire length of the column forimproved vapor -liquid contact. Column length refers to the effective length,measured from the lowest to highest indent in the column.ColumnLength mm15020030045060090012001500Overall Lengthmm300350450600750105013501650ID 19mm24/400102030405060708ID 25mm29/420910111213141516To Order, Call Specialty Glass, Inc. Toll Free 1-800-899-213732ID 25mm35/251718192021222324

DISTILLATION07-1200: DISTILLING HEAD, VIGREUX-CLAISEN - Claisen-type head witha Vigreux column as a side arm. The top is a 10/30which wi ll accommodatea 3” immersion thermometer.Code #Joint 29/4229/42Column Heightmm100200200250300200250300Height X Widthmm250 x 110350 x 110435 x 180475 x 180525 x 180440 x 195490 x 195540 x 19507-1220: DISTILLING COLUMN, OLDERSHAW, PERFORATED PLATE Plain, without jacket. Column consists of a series of sealed-in perforated plates,each with a weir to maintain the liquid level and a downcomer which di rects thereflux to the next lower plate. Ascending vapors pass through the perforationsto form uniform bubbles in a constant depth of liquid flowing across each plate.Withjoints.Code #010203040506070809101112# of Plates5101520304051015203040Plate 1240: DISTILLING COLUMN, OLDERSHAW, PERFORATED PLATE Plain, without jacket. Same as 07-1220 except withjoints.Code #010203040506070809101112# of Plates5101520304051015203040Plate 1228/1228/1228/1250/3050/3050/3050/3050/3050/30To Order, Call Specialty Glass, Inc. Toll Free 1-800-899-213733

DISTILLATION07-1280: LIQUID DIVIDING HEAD, SHELL DESIGN - Magnetically controlledtilting bucket type. Top and bottomjoints are available in either29/42 or50/50. Take-off tube is18/9 and thermometer well is10/30. Vacuumjacketed and silvered to minimize heat loss. Jacket is internally bellowed to allowfor expansion.Code #0102Joint29/4250/5007-1300: COLUMN FEED ADAPTER - For use in providing a feed entrancebetween two distilling columns. Inlet tube as an 18/9 ball joint. Top and bottomjoints are . Thermometer well is10/30. Vacuum jacketed and silvered.Code #0102Joint29/4250/5007-1320: VAPOR DIVIDING HEAD, SHELL DESIGN - Incorporates areversed socket dividing valve that prevents distillate being taken off when valveis closed during reflux cycle. Vapor head is vacuum jacketed and silvered.Allihn type high efficiency condenser is vacuum jacketed. The standard head hasa29/42 column joint, a10/30 thermometer joint andside arm. Furnished with valve rod.Code #01020304050618/9 ball joint onDescriptionComplete Assembly as Shown - 29/42 1” IDComplete Assembly50/50 – 2” IDCondenser Only29/42Condenser Only50/50Vapor Head29/42Vapor Head50/5007-1340: CONDENSER, HIGH CAPACITY - For use with .07-1320 VaporDividing Head. Condenser has an extra cooling coil in addition to the coolingjacket. Vacuum jacketed.Code #0102Description29/4250/50To Order, Call Specialty Glass, Inc. Toll Free 1-800-899-213734

DISTILLATION07-1360: REFLUX CONDENSER, ALLIHN - For use with 07-1280 or 07-1320distilling heads.Code #0102Description29/4250/5007-1350: DC POWER SUPPLYNo Drawing Available07-1380 FLEXOPULSE TIMERA synchronous motor-driven repeat cycle timer used with 07-1400A or 07-1400Belectromagnet. Setting range from .5 seconds to 120 seconds max. 115VAC. 60hz.07-1400-A ELECTROMAGNETFor use with dividing head 07-1320 or 07-1340. 115VAC. 60hz.07-1400-B ELECTROMAGNETDonut style electromagnet for use with dividing head 07-1280. 35VDC.07-1420 DISTILLING HEAD, SHORT PATH: For small quantity distillations.Side and lower joints are the same size. Top thermometer joint is14/20.Code #01020304Description24/4029/4214/2019/2207-1440: DISTILLING HEAD, SHORT PATH, VIGREAUX: For small quantitydistillations. Side and lower joints are the same size. Top thermometer joint is14/20. With Vigreaux indentations for increased surface area.Code #01020304Description24/4029/4214/2019/22To Order, Call Specialty Glass, Inc. Toll Free 1-800-899-213735

DISTILLATION07-1460: DISTILLATE COLLECTOR - Erlenmeyer type flask with slantedbottom. Side arm may be equipped with Teflon or glass plug in stopcock.Code flonJoint24/4029/4224/4029/4207-1480: DISTILLING HEAD – Simple distillation head with a condenser sealed tothe adapter at a 75 angle. The top outer joint on the 14/20 size can be converted toa 10/18 thermometer joint by using a bushing adapter. The side arm is sealed at aheight for use with a 1” immersion thermometer. The inner drip tip joint on thecondenser and inner joint on the uptake tube are the same size.Code #0102Joint24/4029/42Code #03Joint28/120435/2507-1520: DISTILLING HEAD – Dewar style distillation head for use with lowboiling point solvents providing a rapid return of condensed liquid. The reservoircan be charged with dry ice/acetone or liquid nitrogen. Head has a drop counteron the receiver tube and a 10/30 outer joint for use with a 3” immersionthermometer joint. Reservoir has a cooling capacity of approximately 250ml.Available with glass or Teflon stopcocks. Volume of reservoir approximately500ml.Code 0: DISTILLING HEAD, VACUUM TYPE – The position of the cold fingercondenser allows an adjustment of the reflux ratio. Removal of di stillate or areceiver change is possible without interrupting the distillation process due to thepositioning of the stopcocks. The addition of a 0-4mm metering valve in thereceiver arm allows for the regulation of distillate flow. A short water condenseris sealed into the distillate arm. Stopcocks are all 4mm bore Teflon.Code #01020304StopcockGlassGlassTeflonTeflonReplacement ComponentsDistilling Head Only, Stopcocks, 24/40Distilling Head Only, Stopcocks 29/42Cold Finger Condenser Only, 29/42Replacement 4mm PlugJoint24/4029/4224/4029/42Glass Code#05060708To Order, Call Specialty Glass, Inc. Toll Free 1-800-899-213736Teflon Code #09101112

DISTILLATION07-1560: DISTILLING HEAD, VARIABLE REFLUX – The position of the coldfinger condenser allows an adjustment of the reflux ratio. Removal of distillateor a receiver change is possible without interrupting the distillation process dueto the positioning of stopcocks. The addition of a 0-4mm metering valve in thereceiver arm allows for the regulation of distillate flow. A short water condenseris sealed onto the distillate arm. Stopcocks are all 4mm bore Teflon.Code #01020304Column and Receiver Inner Joint Size24/4029/42Approx. Height x Width mm470 x 290475 x 290Replacement 0-4mm Metering PlugReplacement 4mm Teflon Plug07-1580: DISTILLING HEAD, VARIABLE REFLUX joint at top allowsusage of 3” immersion thermometer. A glass stopcock allows the varying of thereflux ratio.Code #010203Joint24/4029/4235.25Please specify eitherorjoints.07-1600: DISTILLING HEAD 10/30 joint allows usage of a 3” immersionthermometer. Stopcocks, either glass or Teflon, permits control of reflux ratioand vacuum. May be operated at either atmospheric or vacuum.Code flonJoint24/4029/4224/4029/4224/4029/42To Order, Call Specialty Glass, Inc. Toll Free 1-800-899-213737

DISTILLATION07-1620: VACUUM DISTILLATION APPARATUS - For use in thedetermination of low pressure distillations of petroleum in accordance withASTM D1160.Code #01020304050607080910DescriptionComplete AssemblyFlask, 500ml, Quartz, T/wellFlask, 500ml, Pyrex, T/wellReceiver, 200ml, GraduatedReceiver, 1000ml, GraduatedElbow AdapterCold Trap, 15ml GraduatedCold Trap, 15ml Graduated with Glass Stopcock.ThermocoupleColumn/Condenser, Silvered, Vacuum Jacketed.07-1640: DIS TILLING HEAD, MAGNETIC CONTROL - Use of anelectromagnetic coil positioning the funnel allows distillate to be taken offinto the receiver or returned to the flask. Stopcock, either glass orTeflon , in the discharge tube allows receivers to be changed withoutinterruption of procedure.Code flonJoint24/4029/4224/4029/4224/4029/42Uses 07-1400B Electromagnet07-1660: DISTILLING RECEIVER, GRADUATED - Supplied with eitherglass or Teflon stopcocks andorjoints. The vacuum connection isabove the graduations and slanted upward.Glass Code 12510Teflon Code 2021222324252627282930To Order, Call Specialty Glass, Inc. Toll Free 1-800-899-213738

DISTILLATION07-1680: DISTILLING RECEIVER - Supplied with either glass or Teflon stopcocks andorjoints. An all purpose receiver enables the user to takecontents of receiver without disturbing the vacuum of the system.Capacityml50ml100ml250mlGlass Code eflon Code 7-1700: DISTILLING RECEIVER, GRADUATED - Supplied with either glassor Teflon stopcocks andorjoints. An all purpose receiver enables theuser to take contents of receiver without disturbing the vacuum of the system.Glass Code 5010203Joint248/40040506Teflon Code oint29/42161718Please specify joint type.To Order, Call Specialty Glass, Inc. Toll Free 1-800-899-213739

DISTILLATION07-1740: DISTILLING RECEIVER WITH ADAPTER – Radial style distillationreceiver allows four flasks to be progressively filled. Upper vacuum adapter isbent at a 105 angle. Complete item consists of a vacuum adapter, distributionadapter, four of the listed size flasks with hooks and ten stainless steel springs.Complete ReceiverCode #Joint SizeReceiver Capacity ml0114/20150219/22150324/4050Replacement Components for 14/20 SizeCode #DescriptionJoint Size04Vacuum Adapter Only14/2005Distribution Adapter Only14/2006Receiving Flasks, 15ml14/2007Springs – Pkg. of 10Replacement Components for 19/22 SizeCode #Description08Vacuum Adapter Only09Distribution Adapter Only10Receiving Flasks, 15ml11Springs – Pkg. of 10Joint Size19/2219/2219/22Replacement Components for 24/40 SizeCode #Description12Vacuum Adapter Only13Distribution Adapter Only14Receiving Flasks, 15ml15Springs – Pkg. of 10Joint Size24/4024/4024/4007-1880: DISTILLING RECEIVER WITH ADAPTER – Radial style distillationreceiver allows four flasks to be progressively filled. Upper vacuum adapter isvertical and hose connection has been replaced by a stopcock. Complete itemconsists of a vacuum adapter, distribution adapter, four of the listed size flaskswith hooks and ten stainless steel springs.Adapter Joints24/4029/42Vacuum AdapterCode #0104Distributing FlaskCode #0205CompleteCode #0306Please Specify Glass or Teflon Stopcock.07-1820: DISTILLING RECEIVER, MOISTURE TEST, BARRETT – Barrettstyle distilling receiver used to determine the water content in petroleum orbituminous material. Receiver is made according to ASTM specifications, withthe addition of the top outer standard taper joint and lower stopcock. The 2mlhas subdivisions of 0.02mL; the 5ml has subdivisions of 0.20mL; the 10ml hassubdivisions of 0.1mL; the 20mL has subdivisions of 0.2 from 0 to 3mL and 0.5from 3 to 20mL. Please specify glass or Teflon stopcocks.Code #010

07-1220: DISTILLING COLUMN, OLDERSHAW, PERFORATED PLATE - Plain, without jacket. Column consists of a series of sealed-in perforated plates, each with a weir to maintain the liquid level and a downcomer which directs the reflux to the next lower plate.