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7upqrpsCN.fm Page 1 Wednesday, November 1, 2000 10:30 AMHP 5973 MSDGCHP 6890
7upqrpsCN.fm Page 2 Wednesday, November 1, 2000 10:30 AMMSDMSDMSDHP 5973 MSDMSDHP 6890GCGCHP 5973HP 6890HP 6890— 2 —GCGC
7upqrpsCN.fm Page 3 Wednesday, November 1, 2000 10:30 intOpenCancelCloseOpen— 3 —
7upqrpsCN.fm Page 4 Wednesday, November 1, 2000 10:30 AMHP 6890GCHP 5973 MSDHP 6890HP 5973 MSDGCMSD— 4 —GC
7upqrpsCN.fm Page 5 Wednesday, November 1, 2000 10:30 AMMSD— 5 —
7upqrpsCN.fm Page 6 Wednesday, November 1, 2000 10:30 AMMSD— 6 —
7upqrpsCN.fm Page 7 Wednesday, November 1, 2000 10:30 AMMSD141— 7 —
7upqrpsCN.fm Page 8 Wednesday, November 1, 2000 10:30 AMMSDView/Instrument Control¿ÉStartRunALS1— 8 —
7upqrpsCN.fm Page 9 Wednesday, November 1, 2000 10:30 AMContentsALSGCGCGCAux 2GC/MSDThermalMSMS— 9 —MS
7upqrpsCN.fm Page 10 Wednesday, November 1, 2000 10:30 AMMS.(.1234).//.Accounts. . .View— 10 —/ Top
7upqrpsCN.fm Page 11 Wednesday, November 1, 2000 10:30 AM/.GCGCGC.(./.).1234MSMS SIM/MSMSMS.1234ViewControl— 11 —/ Instrument
7upqrpsCN.fm Page 12 Wednesday, November 1, 2000 10:30 AMMSMS.Mass #2Mass #3PWDFTPPBFB.Ent.Ent.sMSMS.HelpMSMS I/OMSMS()/./- EIView/ Manual Tune— 12 —
7upqrpsCN.fm Page 13 Wednesday, November 1, 2000 10:30 AM/MSMS I/OMSMS.MSMS.RFPA.MS.MSMSMS./((.()))/View/ Diagnostics/Vacuum Control— 13 —
7upqrpsCN.fm Page 14 Wednesday, November 1, 2000 10:30 AM.(BSB).123.MSGC.ASCII.123.GCGC.View(— 14 —/ Data Analysis)
7upqrpsCN.fm Page 15 Wednesday, November 1, 2000 10:30 AM# /- 2.View/Easy IDCO.QEdit QuantResult— 15 —View/
7upqrpsCN.fm Page 16 Wednesday, November 1, 2000 10:30 AM.(BSB).JCAMPJCAMP.TIC.Parametric Retrieval— 16 —View/
7upqrpsCN.fm Page 17 Wednesday, November 1, 2000 10:30 AMGC/View /AlignGCGC.DAReview Peak PurityView(— 17 —/
7upqrpsCN.fm Page 18 Wednesday, November 1, 2000 10:30 GC/MSD30MSDMSDMSDMSD5955-5398GC45GC/MSDMSDMSD— 18 —MSDMSD
7upqrpsCN.fm Page 19 Wednesday, November 1, 2000 10:30 AMMSD14MSDMSDOK1 MSD GC/MSD10GCGC MSDGC GC/MSD GCGC/15MSD5GC99.999%GC/MSD80%OK*.u MSD23ViewControlVacuumOkay to runMSD6Diagnostics/VacuumMSDPump Down— 19 —2
7upqrpsCN.fm Page 20 Wednesday, November 1, 2000 10:30 AMMSDMSDMSD1InstrumentPerform MS Autotune2OK EMgoodtune.u3— 20 —
7upqrpsCN.fm Page 21 Wednesday, November 1, 2000 10:30 AM— 21 —
7upqrpsCN.fm Page 22 Wednesday, November 1, 2000 10:30 AMMSD1GCInstrument/Inlet/Injection TypesUse n4 1 Misc Info2MethodRunData Acquisition Data Analysis3 1 5100 GCMisc Info6 Acquisition4RunMothedGCRun MethodGCGC— 22 —Wait for GC readyGCPre RunGCStart
7upqrpsCN.fm Page 23 Wednesday, November 1, 2000 10:30 AM11021.0314212567GCStart8— 23 —5
7upqrpsCN.fm Page 24 Wednesday, November 1, 2000 10:30 2Spectrum32[1][1]2Subtract1 1Add[1]Select IntegratorOK12File(BSB)Subtract Background 3 BSB12 [2]— 24 —
7upqrpsCN.fm Page 25 Wednesday, November 1, 2000 10:30 AMTIC12TIC12SpectrumReport3/ Library Search3 Summary4Detailed 45 Difference Statistics Text5Apex,Apex-StartPeakof Peak,Apex-Background at time,AverageOK6Print7DoneChromatogram/Integration Result— 25 —Æ
7upqrpsCN.fm Page 26 Wednesday, November 1, 2000 10:30 ml/minSIMo110 – 20 CoSIMo2ooo— 26 —amuSIM1
7upqrpsCN.fm Page 27 Wednesday, November 1, 2000 10:30 AMGCMSDHP 6890GC/MSDGCGC2— 27 —
7upqrpsCN.fm Page 28 Wednesday, November 1, 2000 10:30 RTRT12345 GC/MSD123412345678910111213— 28 —MSDRT
7upqrpsCN.fm Page 29 Wednesday, November 1, 2000 10:30 AM1234567812345678123456 MSD71234567PFTBASIMMSD123m/z 18,28,324412— 29 —GC
7upqrpsCN.fm Page 30 Wednesday, November 1, 2000 10:30 � 30 —RCF
7upqrpsCN.fm Page 31 Wednesday, November 1, 2000 10:30 AMHP, 30 mm id,85% Vespel 15%graphite,0.4-mm id,85% Vespel 15%graphite,id 0.25-mm id0.5-mm id, 85% Vespel 15% graphite,0.8-mm id, 85% Vespel 15% graphite,0.27-mm id, 90% Vespel 10% graphite,0.37-mm id, 90% Vespel 10% graphite,0.40-mm id, 90% Vespel 10% graphite,0.47-mm id, 90% Vespel 10% graphite,0.74-mm id, 90% Vespel 10% graphite,GC/MSD(/0100-06910.1-mm id0.2-mm0.32-mm id0.53-mm id0.1-mm id0.2-mm id0.25-mm id0.32-mm id0.53-mm 7205971-60571G1099-601770960-0897OOOFNOPFTBA/— 31 —
7upqrpsCN.fm Page 32 Wednesday, November 1, 2000 10:30 AM ,2,3HP 5973 MSD/HP 6890GC, 4MSD,5MSD,6MSD,7,8MS, 10MSD, 18MSD, 19MSD, 20, 22MS, 24, 25, 26GC, 2728, 30, 31, 8/96GCHP 5973 MSD / HP 6890, Rev. A.03.00HP G1701AAG1701-970168/96
HP 6890 GC HP 6890 GC HP 6890 GC MSD 7upqrpsCN.fm Page 2 Wednesday, November 1, 2000 10:30 AM — 3 — . GC 1 Manual 2 GC Run 3 Method Run 4 .
