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.\ · ,. .-":"! .J tJu·,e',,.vPtJu A--FRED C. HART ASSOCI ATES, INC. CONSULTA NTSDENVER FEDERAL CENTER, BUILDING 53. BOX 25227. DENVER. COLO. 80225 (3O3) 234·2883May 24, 1985l eith BradleyUSEPA Region VI1201 Elm StreetFirst International BuildingDallas, TX. 75201COOoDear Mr. Bradley,Enclosed is the original case file for Project 1116F, Bayou Bonfoucha.OPlease sign the space below to indicate receipt of this case file and toserve as chain-of-custody. Return to:FRED C. HART ASSOCIATES, INC.Denver Federal CenterBldg. 53, Box 25227Denver, CO. 80225If you have any questions, please direct them to Linda Bohannon or myselfat FTS 776-0922 or (303) 236-0922.Sincerely,FRED C. HARTASSOCIATES,INC. . ?;,ff } Gloria L. Pol tngOperations AdministratorHazardous Substances LaboratoryReceived by:---- ---- ----Date:*1000323*1000323000783

ENVIRONMENTAL PROTECTION AGENC'\'Office of EnforcementPROJ. NO.?'8L OO"-First International Bldg., 1201 Elm St.CHAIN OF CUSTODYDallis, ,:exas 76270· PROJECT NAMENO.OFREMARKSCONTAINERSSTATION LOCATIONXIfIf,,XRelinquished by: (Sl1/fMtu,.JDate/TimeRelinquishedRelinquished by: (Si,nature}r.Date /Time,Received by: (Sl,,,,.ru,.JRelinquished by:(Si111Mture}Date /TimeReceived by: (Signature)Received by: (Signature}Relinquished by: (Signarurw}Date /TimeReceived by: (Sl,,,,.ru,.JReceived for Laboratory by:Date /Timeef-U"'t'fDistribution: Original AccompMies Shipment; Copy to Coordinatbr Field Files r.r.!:".?en JM AV NIIMRFR000784Remarks(Signature}OF CONTA1Nfm; o ,,"( t,)'f;J().,000784\-

98LOOOU.S. Envll'Olalltal Protection AgencyContract Laboratory Progr PREPARED HAZARDOUS WASTE EXTRACT CUSTODY RECORDiIRegion No.'-\SNO Case No.Regional ContactI/Lt f'-I'e.f 4NEIC Project No.I If, FIV ,4-jRegionStationNumberSupleNllllberftf tlhII'.&1.f. i.&! f·u '3r l'4A{"" 11 ,-JExtracts Preparedo ,.,,CollectionStation LocationDateT1mt!t 11-e. . ,;-lwr"' Ar.,-.,.,- o-S'I/'f '7 ll/J-t.-tI—IJ f 4 n I .If -I' t:If'-Jt,-fjq14 s-" --I/Ctt11AT dI-. C I—. i'/ - R;vu· 5 e,l,·/hf4-t——oDe.,. afL.IX-:i .,.OIo., .,Co.,!iC.oan-a-i.,1VIta enComments.ca.EXXO1X ax'—Total Mercuryduplicate)- . JHazardous Substances Laboratories944 East HannonLas Vegas, Nevada 89109i--XX— Shipped v a F . ,;/ .,. , Ck/'' SAirbill no. 1 'I Z s- i , I, 7;Sealed for shipment «,Relinquished by (signature);;-dJ / /k(/:1.,//.( .000785Datecr-'l-fl'/Datef7'-7'-fd1/I/TimeJ f'JViTimef 1 ·. )c,j'"A.7Received by (signature)DateReceived by (signature)DatelI/tTimeTimeSample Phases:01 Water MisclbleLiquid02 Solid03 Non ter MisclbleLiquid1 /1 /Ri!tfh

l8LOOOHazardous Substances Laboratories944 East HannonU.S. Envlromental Protection AgencyContract Laboratory ProgruLas Vegas. Nevada 89109 ,\Regional ContactI(:,/}"' r f' et I './)4/eSMO Case No.Extracts Prepared.c.,Q/I If r-c,,s-ocuNA:- ,aRegionS.ple.NumberStationF-S"Js-qll A--,-1,AA8·'-·2T t't; P. Station LocationNumber1 I;' CiF 3to,a ,-Ft;'3lllJ 4-C II.----,.,, kIFfi'HISl- lfA-i-"I -c 'Ip- 5" "ID·-2'f'Au,.ur--10-ff tI '1 'f 7000786 A;-.,. ' , " e ,-t.Airbill no. 3 4 J 523 1JJ-/JAf .1,-. Jo- 1.1?K /4,,,,,{ 'Relinquished by (signature), . - I - date J;:rnk/time-3/1'1/t?I "J -: ?0 .date/ timeI ".311t1ls- ?- JoI0 2XX6/0JI.Xlh.XX(J/XX4 I IJ}.xXXOJ.-ixXtJ A (X—I'll.ffi.t? r k""rShipped viaX/;--:Jo- ! II ,;· JL '2. K -c-trir- 'H 7 I 8-,-t,,XA,IIfx// V If,- -' " 4 ,,- .·::'!111,o,,-. .i-!fUl'-/t;-tJ——x"x XReceived by (signature)Received by (signature)CommentsD.t? ");'"-JC-,i'i? · J,- //., .,uIllX .- -f/ i.,.,.s:.Xl'13i'r-,.e,-z:z:cu "OIll .,.'X, - 'J(/-(f 'I Lt"s- X.x.t:.i.J .,,, ';' k:cXIs- Ji0 1'17.o/lurn{CollectionTimeDateS'-lfrfl'f#Jr l'e. -3FS' H. /fl 11 K- - 'IP HtSJ-.,. -.-. -iJ . .,,il., ,, .NEIC Project No.K Pest1c1de/PCBRegion No.WASTE EXTRACT CUSTODY RECORDTCDD Comb.PREPARED HAZARDOUSITCDDI. e Phases:01 Water Miscibleliquid02 Solid03 Nor 'ater Hiscf bleliq . ,d

88LOOOU.S. Envlroiaental Protection AgencyContract Laboratory ProgramI I/. Ff;S.ple:'tulber.,,,1,/Jn /,o/Ju NEIC Project No.A/Af4."' ,. 'I-oCollectionTimeDateStation LocationNumber IanC ,,,,,'::''PIf l" J t::f o'7 t., rr" o t Cl"'A L,"/ AN/IrftP't:t:jC,IftI/cl!?lank.e·' -5; /-' I I . E,t!:.'.L.A Tr" aF18(q"':IQJz.-OJ"'"'o co:cx:i.I::.,"'I--.,"' .QJ.RegionStation.0eC',:,ic;. 0.-u.,.,"'::,I--.OJz:.,,cu -c, JI. uQ.xyyk.coKSMO Case No.Extracts Prepared.,TCDDIbRegional ContactAcid, TCDD-Region No.1Las Vegas, Nevada 89109Piti'AAtu ffAZAROOUS iiASiE EXiRACi tUSiOiYf REtORD--'IHazardous Substances Laboratories944 East Hannono,'Shipped viaAirbill no.Fe,levalf; }(.fflS 3'13-,,;,.31,2.'2-Relinquished by (signature)F:"02,L//(000787lf -tt/J date/,.- t 3Ytldatet-13/time3 ·;. (.:time- rl 1 : ,.lReceived by (signature)dateReceived by (signature)date/I/I1/l/84dhtimetimeSample Phases:01 Water Miscibleliquid02 Solid03 Non Water MiscibleI. uid

µeNumberFieldSampleAqueous LiquidCD@Known or .SampleLlc:ation:·.·. &: 1etUSJf · ·Preparations · Preparation Lab:' SamplingSampling. ·Roc'dBy. · Date Rec'd . 5' - 1@ Inmmation: . .· .(dateI (:t lnoigarlic:s . )'.35:L? ttM ).56· ·.· Total Metals· .Total M··Strong Anions(arbill number)· Specicll l:nstruaticm s:Prep Lab File Copy000788? i ·· ,;,, ./(e.g., broken, leakage,· Chain-of-Custa:iy, etc)Pesticides, FCB(name ofd-Sample Ccmdit:ion on Receipt:te&· tE.t' .,r;. /

Location5Lab:t./Samp)eCoaditian cm 1-teipt:Chmd-0.istcxly, etc.),(e ;./brolam; leakage;I.{;, ( ,!-,,-:,./(. !J'':}:.2: 1 31a'fii :rs,Copy000789

H I G H I C REPORTfllilField SampleAqueous LiquidDate:Sample Location:orOffice:Preparations Requested:·m .,,, -.: (check below).·:·., : ,Shipping:,· ,:,.,,,,: ,,:, . .··,.i.·az· ,. ,. .· Volatile OrganicsBase/Neutral, Acid,·TCDDPesticides, PCBv-:,Inorganicsl- '·Total Metals .35 -:t{6 7/7 3Total MercuryStrong Acid Anbns(airbillnumber)SpecialPrep Lab File Copy000790Preparation Lab:R 'd I:3y[.·. DateRoc"d .· r1),L· ?/ ·'iSample Condition an Receipt:(e.g., broken, leakage, Chain f-Custody, etc.)

Field Sample Sample, geName/Code:oAqueous Liquido.: Oil,.--- - . .; Other:. .or SuspectedSampling Office:(fj-' Preparations Requested:(check below) ·-(begin). -- V61 : ftiQ'2--JiOrtiariici Shipping Jnlonnation:---- Volatile Organts Base/Neutral, Acid, . xf:!)(nameTCDD- Pestic:ides, PCBlnorgaincsi TotalMetalsTotal MercuryStrong Acid Anions S 'Z.3k;-St;173(airbill number)Handling .lnstructicms:.Prep Lab File Copy000791 - Location:,J ffftffi, -w r10) Preparation Lab:Bec'd ytiV. DateRaJ.'cl5? /-C;I/Sample Condition on Receipt:(e.g., broken, leakage, Cpam-of-Custody, efc.)I,c,-tt-rA-

/ pie Number.·r s3s2FIELD SAMPLE REOORD2) Field SampleSample Site Name/Code:Aqueous Liquid)Known or Suspected ' '!,··'.·plingC{)AL'' 7 0R c1?t:;@Tc. Sample. L6cation:i;l)\(.:1\J·ARf r,,· ::., ,.,,. '\;.},:.)Sampling Ped10t111) DO};(phorlf:3):-.(· Sa:mplin tDate: 1,'g,ft,) i ,,,,,,(begin).({:clPreparations(date' .Sample Condition on Receipt:(e.g., broken, leakage, Cl]ain-of-Custody, etc) -; ,.;,. ·:. /MetalsMercuryStrong Acid Anions(airbill Ilumber)Prep Lab File Copy000792Preparation Lab:Sample Volume:(name of;

Field SampleSiteAqueous LiquidOo) ' orSample Location!'SamplingPreparationsSample Condition on Receipt:· · · . . (e.g.; broken, leakage, Chain,of-Custody, etc.)(name of carrier)c::r: -,4 /iHandlingPrep Lab File Copy000793Preparation Lab:

j.··l ·/. · -r,f,i; 'l)'. t: ·; t.i,, ,-.,,. ,;:):-·f/; ,1::t,,,.,;., .,i:. :.-:-.,·-.,, -- .'- · ""0C:::)O. . , ' I.&:at:ion:or Suspected Hazards:(phone),:;,,,Sam. ; :ii''' f'c\;ti,:t, .,. ' . \ J Requested: :-\,;;c1:·.!'. ,'.',·; :'.·( d)·::-· ' ··"· ·.··).fl.-,,.,.;,., ,. · below)··,. v ,Preparation Lab:--·Rec'q By -.,.------ - 1.Jil18: - - - - - - - -c\''·0ateRedd,, -··· - - - -. : -' ,. : ; ', '.'J '.·, - ,-.' ·,.:, '. \.Sample Condition Oil Receipt(e:g.;brokt ti;1eakage}C'hahdD,istody, etc.)(nameI.r0, s:'r·(date shipped) .·. Total Metis- Total MercuryS1rongAcidAnions ·',.,,.'·,,,,,(anpilln ) . , .',,,,'·"!t ::::: ::':s· --, , , . -1:.' "·· :"-,\F,,,,"\Prep Lab File Copy000794

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96LOOO000796

000797

'000798. ''.

c000799

Sample Location:000800

000801

000802

000803

000804

000805

1201 Elm Street CO First International Building Dallas, TX 7520. 1 O o O Dear Mr. Bradley, Enclosed is the original case file for Project 1116F, Bayou Please sign the space below to indicate receipt of this case file and to serve as chain-of-custody. Return to: FRED C. HART ASSOCIATES, INC. Denver Federal 53, Box 25227 Denver, CO. 80225